Material Properties and Processing Open access Peer reviewed

Laboratory Scale vs. Pilot Scale Recyclability Evaluation of a Brown Packaging Paper Containing Strength Additive

Joana C. Vieira, Pedro E. M. Videira, António de O. Mendes, Paula Pinto and 7 more

Recycling | Jun 17, 2026

Abstract

Abstract

Harmonized laboratory methodologies, notably the CEPI recyclability laboratory test method (latest version 3, released February 2025) and the 4evergreen protocol (latest revision 1, released January 2025), are widely used to assess the recyclability of paper-based materials. However, the extent to which laboratory-scale results reflect pilot-scale behavior remains insufficiently documented. In this work, the recyclability of brown packaging paper was evaluated at both laboratory and pilot scales. Disintegration was performed under identical consistency, temperature, and duration, followed by screening, filtrate analysis, macro-stickies quantification, and paper sheet adhesion evaluation according to the CEPI methodology. In parallel, recycled paper prototypes were produced in a pilot paper machine and were mechanically characterized. The material was classified as technically recyclable in a conventional recycling mill at both scales, with closely aligned recyclability scores. Nevertheless, pilot-scale testing revealed higher dissolved and colloidal substances, increased macro-stickies content, and sheet adhesion phenomena not fully apparent at laboratory scale. These results demonstrate that while laboratory tests are robust for recyclability classification, pilot-scale trials provide essential insights into runnability and operational risks relevant for industrial implementation.

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Authors

Researchers on this paper

Joana C. Vieira

first | University of Beira Interior | ORCID 0000-0002-6098-9581

Pedro E. M. Videira

middle | University of Beira Interior | ORCID 0009-0004-0002-6638

António de O. Mendes

middle | University of Beira Interior

Paula Pinto

middle | Pulp and Paper Research Institute | ORCID 0000-0002-1561-4406

Belinda Soares

middle | Pulp and Paper Research Institute

Mariana P. Costa

middle | Pulp and Paper Research Institute

Paulo T. Fiadeiro

middle | University of Beira Interior | ORCID 0000-0002-7374-3636

Joana M. R. Curto

middle | University of Beira Interior | ORCID 0000-0002-5379-7688

Maria E. Amaral

middle | University of Beira Interior

Ana Paula Costa

middle | University of Beira Interior | ORCID 0000-0003-1583-3462

Vera L. D. Costa

last | University of Beira Interior | ORCID 0000-0003-1567-5513

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Citation

BibTeX

@article{Vieira2026Laboratory,
  title = {Laboratory Scale vs. Pilot Scale Recyclability Evaluation of a Brown Packaging Paper Containing Strength Additive},
  author = {Joana C. Vieira and Pedro E. M. Videira and António de O. Mendes and Paula Pinto and Belinda Soares and Mariana P. Costa and Paulo T. Fiadeiro and Joana M. R. Curto and Maria E. Amaral and Ana Paula Costa and Vera L. D. Costa},
  journal = {Recycling},
  year = {2026},
  doi = {10.3390/recycling11060107},
  url = {https://doi.org/10.3390/recycling11060107}
}

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