Catalytic C–H Functionalization Methods
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Abstract
Abstract
A palladium-catalyzed C–H silylation reaction of alkenyl triflates has been developed, employing a norbornene analogue as a relay for C–H activation. The reaction forms C(vinyl), C(alkyl)-palladacycles as the key intermediates via norbornene analogue-relayed C–H activation. These palladacycles subsequently react with a disilane to form disilylated intermediates, which undergo a retro-Diels–Alder reaction to deliver the final products. This method offers an efficient route to Z,Z-1,4-disilylated 1,3-dienes.
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@article{Qiu2026Catalyzed,
title = {Pd-Catalyzed Vinylic C–H Funtionalization for the Synthesis of 1,4-Disilylated 1,3-Dienes},
author = {Xiaoyu Qiu and Dongsheng Yi and Xiang Zuo and Qiongqiong Zhu and Yu Zhang},
journal = {Organic Letters},
year = {2026},
doi = {10.1021/acs.orglett.6c01878},
url = {https://doi.org/10.1021/acs.orglett.6c01878}
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